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The Column
September 21, 2017
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TOP STORY

Determining Chloride and Sugars in Food Samples Using HPLC

Accurate quantification of sugars in saline solution is now possible using a new high performance liquid chromatography (HPLC) method. The Column spoke to Abdelrahman Saleh Zaky from the School of Biosciences at the University of Nottingham (Nottingham, UK) about this method. read more


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FEATURE

Selecting the Best HPLC Column for Carbohydrate Analysis of Food Samples

The various considerations for selecting and optimizing the use of ion-moderated partitioning HPLC analytical columns for carbohydrate analysis in various types of food samples are discussed. read more

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New Publication: Analytix Reporter

From the makers of The Reporter and the makers of Analytix comes... Analytix Reporter. Separation and wet chemistry techniques all in one scientific journal. Whether you are a previous subscriber or want to become a new reader, be sure to fill in your contact details to receive the inaugural edition and all subsequent editions of the new Supelco journal, the Analytix Reporter from MilliporeSigma. www.SigmaAldrich.com/newsletters


Quantitative Comparison of Hormones in Drinking Water Between Low and High Resolution Mass Spectrometry

The quantitative performance of the latest generation of high-resolution instruments is comparable to that of a triple quadrupole MS, even though different scanning modes are used. In an Orbitrap-based instrument, the parallel reaction monitoring (PRM) mode performs most closely to a triple quadrupole mass analyzer using selected reaction monitoring (SRM) mode. This study looks at the performance of an Orbitrap-based LC–MS method for EPA Method 539. read more

INTERVIEW

Analyzing Persistent and Emerging Contaminants in Food

Preventing environmental contaminants from getting in to the food chain is of paramount importance to us all. Yelena Sapozhnikova, a Research Chemist at the Agricultural Research Service, United States Department of Agriculture (USDA) in Wyndmoor, PA, USA, spoke to The Column about her research into the development and evaluation of analytical methods for persistent and emerging organic chemical contaminants in food samples. read more


NEWS

Novel Metabolomics GC Method for Olive Oil Analysis

A method to determine the quality of olive oil has been developed using a novel atmospheric pressure chemical ionization source in combination with gas chromatography coupled to hybrid quadrupole time-of-flight mass spectrometry and a metabolomics strategy. read more

Application Notes

Screening of Pesticides in Food Using GC/Q-TOF

This application note describes the use of a novel high-resolution, low energy EI capable GC/Q-TOF to screen pesticides and other contaminants in food matrices. Read more

mAb Aggregation Using a Cary 60 UV-vis Spectrophotometer

The advantage of UV spectroscopy as an analytical method to detect protein aggregation is that it is non-destructive and uses low sample volumes, minimal sample. Read more

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