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In our July issue:
COLUMNS:
LC TROUBLESHOOTING
Mobile Phase Buffers in Liquid Chromatography
For liquid chromatography (LC) methods where the buffer pH and composition have an influence on retention, which buffer preparation method will provide the most repeatable results? Read more >>
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PHARMACEUTICAL PERSPECTIVES
Bioanalytical Method Validation
The main objective of this review is to provide a clear summary of the different methods that can be used to quantify endogenous small molecules. Practical recommendations to face this bioanalytical challenge, in particular in terms of method validation, will also be given. Read more >>
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Exclusive Videos: Novel Applications for CESI–MS Analysis
At the most recent Global CESI-MS Symposium, researchers explored the use of CESI–MS analysis to characterize monoclonal antibodies, to quantify highly polar pesticides, to identify post-translational protein modifications, to detect pesticide metabolites, and much more.
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GC CONNECTIONS
Temperature Programmed Gas Chromatography
Temperature programming is used for most separations in capillary gas chromatography (GC) today. Despite this, many of the principles by which we understand temperature programmed capillary column separations are based on ideas developed using packed columns and isothermal conditions. This instalment of "GC Connections" dives into temperature programming.
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PEER-REVIEWED ARTICLE:
Sample Treatment in Routine Analysis: Determining Sulphonamides in Liver
A case study related to the determination of sulphonamides in liver is presented. Different extraction strategies, including solid-liquid extraction (SLE), ultrasound-assisted extraction (UAE), and solid-phase extraction (SPE), were evaluated to produce a simple and effective extraction method. Read more >>
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| UPCOMING WEBCASTS |
High-Throughput, Automated Volatiles Analysis from Air, Headspace and Thermal Desorption Tubes
Tuesday, Jul. 23, 2019 at 11am EDT | 8am PDT | 4pm BST | 5pm CEST
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Does Your Electronic Data System Meet 21 CFR Part 11 and CGMP Requirements?
Thursday, Jul. 25, 2019 | North America: 9am EDT | Europe: 3pm CEST | India: 6:30pm IST
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If you would like to submit an article to LCGC, contact Alasdair Matheson, Editor-in-Chief - amatheson@mmhgroup.com.
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