Spectroscopy App Note:
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October 2014 

Featured Application Note:

Thin Film Analysis Using a UV-vis Spectrophotometer and 5 Degree Relative Specular Reflectance Accessory
Shimadzu
Whether multiple or single anti-reflection (AR) coatings are applied to a substrate, it is of critical importance that the individual coatings be analyzed for film thickness prior to making a finished product. This note demonstrates measurement of a single protective coating on an acrylic substrate using UV-vis with a 5 degree relative specular reflectance accessory and film thickness software. Download the PDF
 
Mercury Detection in Coal Samples by Direct Analysis
Sumedh Phatak, Milestone Inc.
This paper describes the importance of mercury analysis in the coal industry and how direct mercury analysis overcomes the challenges faced when analyzing mercury in coal samples using CVAA and ICP.
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Determination of 22 Elements in Copper (Cu)
Dr. Rainer Nehm, HORIBA Scientific
Inductively-coupled plasma-optical emission spectrometry (ICP-OES) easily determines minor and major elements concentrations in copper analysis. This application note describes the development of a method to determine elements in a copper matrix.
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EDXRF Analysis of Silicone Coating on Paper and Plastic
Applied Rigaku Technologies
Paper and plastic are coated with a thin layer of silicone during the manufacture of labels, tape, or other adhesives, or as a barrier coating against air in the packaging of food, medical products, and other materials. EDXRF analysis with the Rigaku NEX QC is shown to be an excellent tool for measuring silicone coating to ensure the proper physical properties of the product are maintained.
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Miniature 60 kV, 1000 µA, 12 W X-ray Source
Sterling Cornaby, Moxtek
The new 12 W source from Moxtek is meant for use in small beach top and portable XRF systems where small size components are valued. Its features are critical for more precise and faster XRF analysis of heavy and light elements at low concentrations.
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Analysis of Gemstones and Diamonds in Jewelry using FTIR Microscopy
Thomas J. Tague Jr., PhD, Bruker Optics, Inc.
The LUMOS FTIR microscope is suitable for the examination, identification, and classification of mounted diamonds.  Small stones that are in close proximity to others can be used to readily determine whether the stone is natural or synthetic and whether it has undergone treatment, thereby assessing its true value.
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Using the Full Spectrum for Raman: from UV to NIR
Dr. E. Illy, Professor W. R. Browne, and Dr. A. Draksharapu, Cobolt
With the current availability of high performance DPSS lasers offering a broad range of wavelengths from the UV to the NIR, the applications for Raman spectroscopy are only just beginning to be fully explored.
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Raman Imaging in Life Science - Cells, Bacteria, and Tissues
WITec
The whitepaper provides information about Raman imaging in life science. It covers:
  • Cells, bacteria, tissue
  • Substance distribution in cells and tissue
  • Investigations of cancer tissue
  • Combined Raman-AFM and Raman-SEM analysis
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Analysis of Artificially Weather PET and a Separate PET Hydrolysis Evaluation Using the 4300 Handheld FT-IR
Frank Higgins, Pik Leung Tang, and Alan Rein, Agilent Technologies
Elucidating chemical changes in carbon fiber composites prior to physical degradation has been effectively demonstrated using handheld FT-IR analyzers. This application note shows that a handheld infrared spectrometer is equally effective at measuring early onset chemical changes in environmentally stressed PET polymer, which precede cracking and other physical degradation processes. This is an important issue in applications where polymers (as well as other materials such as paints and coatings) are exposed to environmental conditions varying from climatic conditions that depend on their geographic locale to complete submersion, as in the case of marine paints. The commercial availability of handheld FT-IR spectrometers affords the capability of nondestructively measuring areas of large polymer sheets, as well as other coatings.
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Rapid Crystal Orientation
Owen Vajk and Don Bilderback, Multiwire Laboratories
The MWL120 real-time Laue camera combines single-photon detector sensitivity, rapid signal processing technology, and innovative software control to provide the fastest, easiest way to orient single crystals.
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Augmenting Standard Methods of Measuring Airborne PM2.5 Using IR Imaging
Mitsuhiko Morimoto, PerkinElmer
Global concern is growing over the amount of pollution in the atmosphere and the effect on human health. Learn how to measure PM2.5 by the use of imaging FT-IR microscopy.
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Narrowband Laser Characterization
Ocean Optics
Miniature spectrometers can be configured to characterize high-resolution laser output in the UV-vis and NIR spectral regions, either as part of an internal laser feedback loop or externally.
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Nanoscale IR spectroscopy: Analyzing Polymer Composites
Curt Marcott, PhD and Mike Lo, PhD, Anasys Instruments
Polymer composites are a very important class of materials where new components such as fibers, nanotubes, clays and so on, are added to polymer matrices to enhance properties and add value to the product. Understanding the interphase of the composite and polymer matrix is important to optimize the processing conditions and to understand degradation or other failure mechanisms. AFM-IR is a new technique wherein an atomic force microscope (AFM) probe tip is used as an IR absorbance detector to provide nanoscale IR spectroscopy. This article discusses the application of AFM-IR to provide nanoscale chemical and physical property information about a carbon fiber/epoxy composite.
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Analysis of Polluted Soil by TG-IR Technique
M.G. Garavaglia, PerkinElmer
A challenging analytical problem with increasing importance is the analysis of soil polluted by the dispersion of organic fluids which sometimes features particularly high boiling points.
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